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Chemistry 1909

The Synthesis of Ammonia from its Elements

Fritz Haber (with Carl Bosch)

Forcing air's inert nitrogen into ammonia made fertiliser from the sky — feeding billions, and arming a war.

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In depth · the introduction

The air is four-fifths nitrogen, yet crops can starve for it. Haber found a way to grab that nitrogen out of the sky.

The big idea

Every plant — and so every animal and person — needs nitrogen to build proteins and DNA. The strange thing is that we are swimming in it: nitrogen makes up about 78% of the air. But that air-nitrogen, N₂, is locked up in a molecule so stable that almost nothing alive can pry it apart and use it.

Fritz Haber found a way to force it open. Under great pressure and heat, with the help of a metal that speeds the reaction along, nitrogen from the air joins with hydrogen to make ammonia — the raw material of fertiliser. For the first time, the nitrogen plants need could be manufactured from thin air, instead of dug out of the ground.

How it came about

By 1900 the world had a quiet crisis brewing. Crops were fertilised mainly with nitrate mined in Chile and seabird droppings, and the chemist William Crookes had warned that these were running out — that the growing population might outstrip its food. Whoever could pull nitrogen from the air would feed the world.

Around 1909 Haber, in Karlsruhe, built a small high-pressure apparatus that did exactly that, producing a steady trickle of ammonia. The chemical company BASF bought the idea, and there the engineer Carl Bosch performed a second miracle: he scaled a delicate bench reaction up into giant steel vessels that could survive the crushing pressures, and a colleague found a cheap iron catalyst to replace Haber's rare metals. The first factory opened in 1913. But the story has a dark second half: Haber threw himself into Germany's war effort, becoming the father of poison-gas warfare, and the same reaction that made fertiliser also made the nitrates for explosives. He won the Nobel Prize in 1918 to international outrage, and — himself Jewish — was later driven out of Germany by the Nazis.

Why it mattered

It is hard to name a single chemical reaction that changed more lives. By making fertiliser cheap and abundant, Haber–Bosch let farms feed billions of extra people; a common estimate is that around half the people alive today are fed thanks to it. And the very same power over nitrogen armed a century of war. It is the clearest case we have of a discovery that is both indispensable and dangerous.

A way to picture it

Imagine two dancers who are perfectly happy alone and refuse to take a partner — that's nitrogen's tight N₂ pair. To get them to swap partners with hydrogen, you crowd the dance floor (high pressure pushes them together) and you hire a matchmaker who introduces them without being used up (the catalyst). Heat speeds everyone up, but too much heat and the new couples split again — so you settle on a careful middle temperature. Crowd them, warm them just enough, and keep recycling the wallflowers, and a steady stream of new pairs — ammonia — walks off the floor.

Interactive ammonia equilibrium: two sliders set temperature and pressure for nitrogen plus hydrogen turning into ammonia; the bar shows what fraction of the gas becomes ammonia, rising when you raise the pressure and falling when you raise the temperature.

Where it sits

This is industrial chemistry's first great triumph, standing on the equilibrium ideas of Gibbs and on Le Chatelier's principle, and on the atomic chemistry of Dalton, Avogadro and Lewis already in this Library. It answered the nitrogen-famine fear of its day — and it set the template for the high-pressure catalytic processes that the twentieth-century chemical industry was built on.

The original document
Original source text
Fritz Haber · Nobel Lecture, Stockholm · 2 June 1920 · "The Synthesis of Ammonia from its Elements"
The reaction
Gaseous nitrogen combines with gaseous hydrogen in simple quantitative proportions to produce gaseous ammonia.
[Editorial summary] The lecture then stresses that this union is reversible and never complete: at any temperature and pressure the gases settle into a chemical equilibrium — a fixed fraction of ammonia coexisting with unreacted nitrogen and hydrogen — and the whole industrial problem is how to make that fraction large and reach it fast.
Equilibrium versus rate
[Editorial summary] Haber recounts measuring the equilibrium and finding it discouraging: because the reaction gives out heat and shrinks four gas molecules into two, ammonia is favoured by high pressure and low temperature, yet at the low temperatures the equilibrium prefers, the gases react impossibly slowly. The way through was a catalyst — he reports finding osmium, then uranium, effective — run under high pressure, with the unreacted gas recirculated again and again so that small per-pass yields accumulate.
From bench to industry
[Editorial note] Haber's 1909 table-top apparatus, built with his assistant Robert Le Rossignol, produced a steady drip of liquid ammonia and was demonstrated to BASF. Carl Bosch and Alwin Mittasch then turned it into the first large-scale high-pressure chemical industry — pressure-bearing steel reactors and a cheap promoted-iron catalyst that is still used — and the first factory opened at Oppau in 1913.
[ … ]
Karlsruhe & Stockholm · 1909–1920